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SYNTHESIS AND CHARACTERIZATION OF THE Td-TYPE CLATHRATES: M(2,2- DIMETHYL-1,3-DIAMINOPROPANE)M'(CN)4.2C6H6 (M= Mn or Cd, M'= Cd, Hg or Zn)
(2017)Mn(DMPDA)M(CN).2C6H6Cd(DMPDA)M(CN)4.C6H6 (M= Cd or Hg) Hofmann-Td-type clathrates were synthesized and characterized by vibrational spectroscopy. Infrared spectra of Mn(DMPDA)M(CN)4.2C6H6 (M = Cd, Hg or Zn; DMPDA = ... -
Synthesis and characterization of veratryl alcohol imprinted and nonimprinted methacrylamido polymers
(Scientific Publishers India, 2016)In this study, the synthesis and structural properties of a Molecularly Imprinted Polymer (MIP) and a Nonimprinted Polymer (NIP) bearing Fe-porphyrin moiety and amino acid moieties including Histidine (His), Tryptophan ... -
Synthesis and characterization, novel across adjacent ring formed phthalocyanine
(Royal Soc Chemistry, 2011)Novel mononuclear Zn(II) 4, Co(II) 5 and Cu(II) 6 metallophthalocyanines have been synthesized from 4,4'(ethane-1,1-p-phenol-2,2-p-phenoxy) phthalonitrile 3, which can be obtained by the reaction of 4-nitrophthalonitrile ... -
Synthesis and crystal structure of cyano-bridged three dimensional polyheteronuclear complex
(Walter De Gruyter GMBH, 2012)The cyano-bridged 3D heteronuclear polymeric complex, [Cd(NH3)(mu-ampy)Ni(mu-CN)(4)](n), (1) (ampy = 3-aminomethylpyridine), has been synthesized and characterized by FT-IR and Raman spectral, thermal and elemental analyses. ... -
Synthesis and electrochemical polymerization of a novel 2-(thiophen-2-yl)-4-(thiophen-2-ylmethylene)oxazol-5(4H)-one monomer for supercapacitor applications
(Elsevier Science BV, 2016)In this study, the organic synthesis, electrochemical polymerization and electrochemical characterization of a novel 2-(thiophen-2-yl)-4-(thiophen-2-ylmethylene)oxazol-5(4H)-one, 3, monomer have been reported for supercapacitor ... -
Synthesis and non-linear optical properties of monopyrrolotetrathiafulvalene derived donor-pi-acceptor dyads
(Royal Soc Chemistry, 2004)The synthesis of novel donor-pi-acceptor dyads based on a pyrrolo-annelated tetrathiafulvalene unit is described. The linear and non-linear optical properties of these chromophores have been investigated, together with ... -
Synthesis and Photodiode Characterization of Novel Twisted Carbazole Derivatives with 1,3,5-Benzene Core
(Springer, 2018)In this study, considering the information given in the literature the Ullman and Suzuki-Miyaura coupling reactions were carried out using carbazole, 1,3,5 tribromo benzene and aryl boronic acid. The synthesized novel ... -
Synthesis and spectroscopic characterization of new Schiff bases containing the benzo-15-crown-5 moiety
(Molecular Diversity Preservation International, 2004)New crown ether Schiff base derivatives were prepared by the condensation of 4'-formylbenzo-15-crown- 5 or 4'-formyl-5'-hydroxybenzo-15-crown-5 with 1,2-bis(2aminophenoxy)ethane. The structures of these new compounds were ... -
Synthesis and Spectroscopic Characterizations of Novel Ni(Ii) and Co(Ii) Dithiophosphinate Complexes, and X-Ray Studies on the Ni(Ii) Complex
(Taylor & Francis LTD, 2012)The reaction of 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide (Lawesson's Reagent) with two different Grignard reagents gave the corresponding dithiophosphinic acids (DTPA), CH3OC6H4-(R)P(S)SH; [R = ... -
Synthesis and Structural Characterization of Pyrrole Heterocyclic Systems Bearing Amino Acid Units: Novel Pyrrol-3-ones, Pyrrolo[1,2-a][3,1]benzoxazines, and Pyrrolo[2,1-b][1,3]oxazoles
(Wiley-Blackwell, 2014)Furan-3-one derivatives 1 were converted into 2-hydroxy-pyrrole-3-ones 4 by reacting with various - and -amino acids. In contrast, the reaction of furan-3-ones and 1-aminocyclobutanecarboxylic acid afforded spiro-pyrrolo ... -
Synthesis and theoretical study of bis(fluoroisatinato)mercury(II)
(Elsevier Science BV, 2009)Bis(fluoroisatinato)mercury(II) was synthesised from the reaction between 5-fluoroisatin (HFI) and mercury(II) acetate in methanol. Mercury(II) coordination with nitrogen atom of 5-fluoroisatin molecule was observed using ... -
Synthesis and vibrational spectroscopic analysis of some Hofmann type clathrates
(Pergamon-Elsevier Science LTD, 2011)New Hofmann type clathrates in the form of M(pp)(2)Ni(CN)(4)center dot 2G (where pp = 1-phenylpiperazine, G = 1,4-dioxane and M = Ni, Co or Cd) have been prepared in powder form and their FT-IR and FT-Raman spectra are ... -
Synthesis characterization and biological activity of mixed ligand silver(I) complex of 2-benzimidazolylurea and triphenylphosphine
(Pergamon-Elsevier Science LTD, 2017)The treatment with triphenylphosphine (TPP) in DMF solution of the white precipitation derived from the reaction of silver(I) nitrate with 2-benzimidazolylurea (BZIMU) results in the [Ag(TPP)(2)(BZIMU)NO3] (1) complex. The ... -
Synthesis of 4-hydroxyquinoline-2,3-dicarboxylates using N-(2-aminobenzoyl)benzotriazoles
(Pergamon-Elsevier Science LTD, 2017)A method for the preparation of 4-hydroxyquinoline-2,3-dicarboxylates has been developed by aza-Michael addition reaction of N-(2-aminobenzoyl)benzotriazoles with dimethyl acetylenedicarboxylate. 4-Hydroxyquinoline-2,3-d ... -
Synthesis of 5-(4-methacrylamidophenyl)-10,15,20-triphenylporphyrin, its copolymerization with acrylamide and EDMA, use of this copolymer in the adsorption of bovine serum albumin
(Elsevier Science BV, 2007)A rigid and porous polymeric adsorbent was prepared from monomers 5-(4-methacrylamidophenyl)-10,15,20-triphenylporphyrin (1%), acrylamide (39%), and cross-linking agent ethylene glycol dimethacrylate (60%) using suspension ... -
Synthesis of an F-BODIPY [2]catenane using the chemistry of bis(dipyrrinato) metal complexes
(Royal Soc Chemistry, 2017)ML2 type complexes of an olefin terminated 5H-dipyrrin ligand can be subjected to twofold ring closing metathesis to give bis(dipyrrinato)copper(II) and bis(dipyrrinato) zinc(II) [2] catenates. Demetalation of the copper(II) ... -
Synthesis of cholesterol imprinted polymeric particles
(Elsevier Science BV, 2007)The aim of this study is to prepare cholesterol-imprinted polymeric particles. N-Methacryloyl-(L)-tyrosinemethylester (MAT) was chosen as the complexing monomer. In the first step, functional monomer MAT was synthesized ... -
Synthesis of ferrocene substituted dihydrofuran derivatives via manganese(III) acetate mediated radical addition-cyclization reactions
(Pergamon-Elsevier Science LTD, 2017)In this study, the manganese(III) acetate mediated radical addition-cyclization reactions of ferrocene substituted alkenes and active methylene compounds were carried out. The regio- and stereoselective radical cyclization ... -
Synthesis of new bis-bidendate N/O spiro-bino-spiro-cyclotriphosphazenes: Structural investigations and DFT studies
(Taylor & Francis LTD, 2017)The Schiff bases 4,4'-di(2-hydroxybenzyl imino) diphenylmethane (S1), 4,4'-di(2-hydroxy-5-chloro benzyl imino) diphenylmethane (S2) and 4,4'-di(2-hydroxy-5-bromo benzyl imino) diphenylmethane (S3) were synthesized from the ... -
Synthesis of New Phosphorus Ylides: Spectroscopic and X-ray Structural Studies
(John Wiley & Sons Inc, 2010)Stable phosphoranes, Ar(3)P = CHCOR (R = C(6)H(5), C(6)H(4)NO(2), C(6)H(4)OCH(3), CH 3, OCH(2)C(6)H(5); Ar = p-tolyl or phenyl), have been C-acylated by acetic anhydride to obtain new types of phosphorus ylides. Synthesis ...