Crystal structure of [1-(1H-benzoimidazol-2-yl)-ethanone thiosemicarbazone]2nickel, [C20H22N10S2Ni]

Abstract

The title compound, [C20H22N10S2Ni], crystallizes in the triclinic space group P1 with cell parameters a = 10.9319(9)Å, b = 12.0083(9)Å, c = 13.4978(11)Å, ? = 87.057(7)°, ß = 85.841(7)°, ? = 63.820 (6), V = 1585.6(2)Å3, Z = 2. The structure was refined to a final R value of 0.0498 for 4798 reflections [I > 2?(I)]. The nickel atom is in a regular octahedral environment by four nitrogen atoms and two sulfur atoms. 2005 © The Japan Society for Analytical Chemistry.